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This section provides a number of examples to illustrate approaches to the identi cation of unknown organic materials by using infrared spectroscopy. First, an example of the use of the technique in identifying an organic compound containing a number of functional groups is provided. Citronellal is the terpenoid responsible for the characteristic aroma of lemon oil, and is used in perfumes and as a mosquito repellent. The infrared spectrum of citronellal is shown in Figure 4.11. At the higher-wavenumber end of the spectrum, the C H stretching region provides important information about the citronellal structure. This region is intense, hence indicating the presence of a number of C H groups in the structure. Distinct C H stretching modes at 2800 and 2700 cm 1 appear at wavenumbers characteristic of aldehydes. In addition, a strong band at 1730 cm 1 con rms the presence of an aldehyde group. The other C H stretching modes appear in the 3000 2900 cm 1 range and can be attributed to aliphatic C H stretching. The lack of bands at wavenumbers greater than 3000 cm 1 suggests that there is no aromatic group in the citronellal structure. The structure of citronellal is illustrated in Figure 4.12.

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A unique attempt to conduct a polygraph study in a realistic setting and maintaining certainty about the ground truth was made by Ginton, Daie, Elaad, and Ben-Shakhar (1982) The participants in this study were 21 Israeli policemen who took a paper-and-pencil test that was presented as a requirement for a police course in which they were enrolled They were asked to score their own tests, which provided an opportunity to cheat by revising their initial answers However, the test answer sheets were chemically treated so that cheating could be detected It turned out that seven out of the 21 participants cheated Later, all were told that they were suspected of cheating They were offered a polygraph examination, and were told that their future careers in the police force might depend on the outcome of this examination.

(The option to allow the police of cers to refuse to take the test was realistic As mentioned before, in criminal investigations taking a polygraph test is an option and not a requirement for a suspect) Although initially all 21 policemen agreed to undergo a polygraph examination, one guilty of cer did not turn up for the actual examination, and two (one guilty and one innocent) refused to take the polygraph test Three other guilty participants confessed just before the polygraph interrogation,18 so the nal sample included only two guilty and 13 innocent participants The CQT was used, and the outcomes were rather accurate Both guilty of cers were accurately detected, but two of the 13 innocent of cers were mistakenly judged to be lying Although the ndings appear to give impressive support for the CQT, in fact they do not.

r linking of resources r linking of services into aggregate ones r dependencies between components.

The examiner who made the decisions about guilt and innocent of the examinees had access to both polygraph data and the participants general demeanour during the examination His accuracy with regard to innocent participants.

This syntax form is available to all the commands in this chapter that name a column or table. You can even use it to refer to a specific column in a table, such as test_db.customer.name.

1 Peel the potatoes and cut into 2-inch (5-centimetre) pieces. 2 Place the potatoes and garlic in a medium saucepan and add just enough water to cover

in which k0 is the free space wave number, and n x; y; z is the inhomogeneous index of refraction. As in Section 12.3, the variation of n x; y; z is written as n x; y; z " n x; y; z n 20:2-4

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electronic con guration, 21 lanthanide multidentate ligands, 21 multidentate ligand effect, 21 tungsten(IV), 21 Inherent conductivity, 215 Initiators for chain polymerizations anionic, 59, 68 69 cationic, 59, 65 68 radical, 59 65 azo, 60 61 electrochemical, 64 65 iron(II) plus H2 O2 , 61 peroxo, 60 61 persulfates plus reductants, 60 photolytic, 61, 63 64 polysilanes, 61, 63 silver alkyls, 60 61 Inorganic polymers, de nitions, 2 3 Insolubility of metal-containing polymers, 21, 40, 84 overcoming, 41 52, 84 85, 87 Insulator conductivity, 213 214 Interface coupling reactions, 186 192 chromium coupling agents, 192 silicon coupling agents, 186 188, 194 titanium coupling agents, 188 zirconium coupling agents, 188 192 Intervalence charge transfer spectra, 142 143, 151 152 exercise, 178 Intractability, see Insolubility Iron(II) coordination polymers 2,5-dioxoquinonate, 14 15 oxalate, 14 15 5-phenyltetrazole, 13 14 shish kebob conductivities, 215 Iron(II) magnetic changes vs. temperature, 223 224 Iron M ssbauer spectra, 161 165 o

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